CAS No.: | 5943-30-6 |
---|---|
Formula: | C8h18s2 |
EINECS: | 227-702-1 |
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SEC-butyl disulfide Quick Details
Chemical Name: sec-butyl disulfide
Synonyms: Di-Sec-butyl disulfide, bis(sec-butyl) disulphide
CAS-No.: 5943-30-6
MolecularFormula: C8H18S2
Molecular Weight:176.36g/mol
Density: 0.957 g/cm3
Melting point:-49°C
Boiling point: 220.6°C
Flash point:67.2 °C -closed cup
Solubility: Soluble in ethanol and ether, insoluble in water.
SEC-butyl disulfide Typical Properties
Item | Index |
Appearance | Colorless liquid |
Purity | 98.5%min |
Water | 0.1%max |
SEC-butyl disulfide Usage
This product is mainly used as an organic intermediate.
SEC-butyl disulfide Packaging
180 kg/drum, or according to the customer's request.
SEC-butyl disulfide Storage
Keep airtight in a dry and cool place.
SEC-butyl disulfide Preparation or source
(1) The corresponding bromobutane and sodium sulfide were refluxed into ethanol.
(2) The corresponding butanol and carbon disulfide were heated and refluxed.
(3) Using corresponding butanol and hydrogen sulfide as raw materials, heated under the catalysis of gamma-alumina, prepared by gas-solid catalytic reaction.
A Small Method for Preparing Disec-Butyl Disulfide
1. Sodium sulfide and water were added into the reaction bottle, after stirring and dissolving, sulfur powder was added, heated to 55 C under stirring for 1 hour, then cooled.
2. The microwave reactor was opened and stirred for 0.2-2 hours at 300-1000W power to terminate the reaction. Disec-butyl disulfide was synthesized from the reaction liquid by standing, separating the water phase, and distilling the organic phase.
Remarks
Isomers of dibutyl sulfide. It's stimulating.
SEC-butyl disulfide Packaging and Shipping
Packing: 25Kg/drum
Delivery: Delivery within 3-5 working days.
SEC-butyl disulfide Storage
Avoiding light and drying.